三步萃取法测定水泥中方镁石的含量任务书
2020-06-04 20:26:14
1. 毕业设计(论文)的内容和要求
1、 查阅文献:使用中文数据库(例如中国期刊网、维普、中国博士学位论文全文数据库等)、外文数据库(例如acs、elsevier、web of science等)查阅关于水泥和混凝土中方镁石对安定性影响以及方镁石定量测定等方面的文献。
2、 撰写文献综述; 3、设计实验方案并准备原材料; 4、完成开题报告; 5、 完成1篇英文文献的翻译; 6、 进行试验工作,并及时整理、分析和总结实验结果; 7、撰写毕业论文,完成毕业答辩工作。
论文中并附有描述和总结。
2. 参考文献
[1]Taylor H F W. Distribution of sulfate between phases in Portland cement clinkers[J]. Cement Concrete Research, 1999, 29(8):1173-1179. [2]Twomey C, Birkinshaw C, Breen S. The identity of the sulfur-containing phases present in cement clinker manufactured using a high sulfur petroleum coke fuel[J]. Journal of Chemical Technology and Biotechnology, 2004, 79(5):486-490. [3]Greer W L. Interactions Among Gaseous Pollutants from Cement Manufacture and Their Control Technologies[J]. R D Serial, 2003, 2728. [4]李小燕, 胡芝娟, 叶旭初,等. 水泥窑烧高硫煤的难点问题探讨[J]. 硅酸盐通报, 2010, 29(2):377-383. [5]刘江. 稀醋酸溶液萃取回收工艺研究[D]. 中国石油大学(华东), 2011. [6]李伟峰, 王京刚, 侯贵华,等.水杨酸溶液萃取转炉钢渣中硅酸盐相的研究[J]. 硅酸盐通报, 2008, 27(2):365-369. [7]李召峰, 周宗辉, 单立福. 氢氧化钾-蔗糖溶液(KOSH)萃取钢渣中间相的研究[C]. 中国硅酸盐学会水泥分会首届学术年会论文集. 2009. [8]唐明述, 袁美栖, 韩苏芬,等. 钢渣中MgO、FeO、MnO的结晶状态与钢渣的体积安定性[J]. 硅酸盐学报, 1979(1):37-48. [9]Furrer G, Stumm W. The coordination chemistry of weathering: I. Dissolution kinetics of δ- Al2O3, and BeO[J]. Geochimica Et Cosmochimica Acta, 1986, 50(9):1847-1860. [10]Gutteridge W A. On the dissolution of the interstitial phases in Portland cement[J]. Cement Concrete Research, 1979, 9(3):319-324. [11]Arjunan P, Kumar A. Rapid techniques for determination of free lime and free magnesia in cement clinker and portlandite in hydrates[J]. Cement Concrete Research, 1994, 24(2):343-352. [12]Aldridge L P. Accuracy and precision of an X-ray diffraction method for analysing portland cements[J]. Cement Concrete Research, 1982, 12(4):437-446. [13]Rietveld H M. A profile refinement method for nuclear and magnetic structures[J]. Journal of Applied Crystallography, 1969, 2(2):65-71. [14]Rietveld H M. Line profiles of neutron powder-diffraction peaks for structure refinement[J]. Acta Crystallographica, 1967, 22(1):151-152. [15]Alexander L, Klug H P. Basic Aspects of X-Ray Absorption in Quantitative Diffraction Analysis of Powder Mixtures[J]. Powder Diffraction, 1948, 4(2):66-69. [16]Chung F H. Quantitative interpretation of X-ray diffraction patterns of mixtures. I. Matrix-flushing method for quantitative multicomponent analysis[J]. Journal of Applied Crystallography, 1974, 7(6):519#8211;525. [17]单小兵, 张其土, 李玉华. X射线K值法在水泥物相中的应用[J]. 理化检验-物理分册, 2002, 38(8):342-345. [18]Katyal N K, Ahluwalia S C. Rapid Estimation of Free Magnesia in OPC Clinker and 3CaO:1SiO2 System by Complexometry[J]. Cement Concrete Research, 1998, 28(4):481#8211;485. [19]Bish D L, Post J E. Quantitative Mineralogical Analysis Using the Rietveld Full-Pattern Fitting Method[J]. American Mineralogist, 1993, 78(9):932-940. [20]陈福松, 徐玲玲, 张志宾,等. 水泥熟料中方镁石定量分析[J]. 硅酸盐通报, 2009, 28(6):1295-1299. [21]宋清编. 定量分析中的误差和数据评价[M]. 高等教育出版社, 1982.
3. 毕业设计(论文)进程安排
2016/12/5-2017/1/13 查阅文献,外文文献翻译,文献综述和开题报告的撰写 2017/3/20-2017/4/28 进行实验 2017/5/2-2017/5/5 中期答辩 2017/5/6-2017/6/1 在前阶段工作的基础上,按照计划进行试验工作; 2017/6/2-2017/6/9 撰写毕业论文 2017/6/10 毕业答辩