三维有序介孔氧化锰的制备及性能研究任务书
2020-06-08 21:15:29
1. 毕业设计(论文)的内容和要求
本次论文的完成主要有以下要求:查阅相关文献资料,能够读懂英文文献;综合文献中的实验方法,设计与课题相关的条件实验;开展各个不同的条件实验,在实际操作过程中要能够分析并解决突发问题,能够对不同的实验结果进行分析对比;通过红外、核磁光谱对目标产物进行鉴定,能够对谱图进行分析;最后完成撰写本课题论文的任务。
2. 参考文献
[1] Chu A, Braatz P. Comparison of commercial supercapacitors and high-power lithium-ion batteries for power-assist applications in hybrid electric vehicles: I. Initial characterization [J]. Journal of Power Sources, 2002, 112(1): 236-246. [2] Conway B E, Birss V, Wojtowicz J. The role and utilization of pseudocapacitance for energy storage by supercapacitors [J]. Journal of Power Sources, 1997, 66(1-2): 1-14. [3] Pell W G, Conway B E, Adams W A, Oliveira J. Electrochemical efficiency in multiple discharge/recharge cycling of supercapacitors in hybrid EV applications [J]. Journal of Power Sources, 1999,80(1-2):134-141. [4] Conway B E. Electrochemical supercapacitors [M]. New York,Kluwer Academic/Plenum Publishers, 1999. [5] Zhao D, Feng J, Huo Q, et al. Triblock copolymer synthesis of mesoporous silica with periodic 50 to 300 angstrom pores [J]. Science, 1998, 279 (5350): 548-552. [6] Yang C M, Sheu H S, Chao K J. Templated synthesis and structural study of densely packed metal nanostuctures in MCM-41 and MCM-48 [J]. Advanced Functional Materials,2001, 12: 143-148. [7] Tian B Z, Liu X Y, Yang H F, et al. General synthesis of ordered crystallized metal oxide nanoarrays replicated by microwave-digested mesoporous silica [J]. Advanced Materials,2003, 15 (16): 1370-1374. [8] Jiao F, Bruce P G. Mesoporous crystalline β -MnO2: a reversible positive electrode for rechargeable lithium batteries[J].Advanced Materials Mate, 2007, 19: 657-660. [9] Kleitz F, Choi S H, Ryoo R. Cubic Ia3d large mesoporous silica:synthesis and replication to platinum nanowires, carbon nanorods and carbon nanotubes [J]. Chem Commun, 2003,2136-2137 [10] 张莹,刘开宇,张伟,等.二氧化锰超级电容器的电极电化学性质[J]. 化学学报, 2008, 66(8): 909-913. [11] 邢伟,李丽, 阎子峰,等. 介孔氧化镍的合成、表征和在电化学电容器中的应用[J]. 化学学报, 2005,63 (19): 1775-1781. [12] X. F. Tang, J. L. Chen, X. M. Huang, Y. D. Xu, W. J. Shen, Appl. Catal. B,2008, 81,115. [13] B. Y. Bai, H. Arandiyan, J. H. Li, Appl. Catal. B, 2013, 142#8211;143, 677. [14] X. Wang, Y. D. Li, J. Am. Chem. Soc., 2002, 124, 2880. [15] C. Wang, L. Sun, Q. Q. Cao, B. Q. Hu, Z. W. Huang, X. F. Tang, Appl. Catal. B, 2011, 101, 598. [16] A. E. Espinal, L. C. Zhang, C. H. Chen, A. Morey, Y. F. Nie, L. Espinal, B. O. Wells, R. Joesten, M. Aindow, S. L. Suib, Nat. Mater., 2010, 9,54.
3. 毕业设计(论文)进程安排
2017.3.1-2010.3.15 查阅文献资料, 在此过程中包括开题报告的完成 2017.3.15-2017.4.1 设计条件实验 2017.4.1-2017.5.30 开展各类条件实验, 在此过程中包括对实验产物的红外、核磁谱图分析 2017.5.30-2017.6.15 撰写论文