1. 毕业设计（论文）的内容和要求

内容：利用射流膜乳化技术，使用非对称的管状陶瓷膜作为乳化介质，在较高的压力下，在乳液粒径和乳化通量之间的矛盾之中寻找到既满足乳液粒径要求，又能达到更大通量的实施方案。

要求：（1）熟练掌握陶瓷膜的表征手段； （2）熟练掌握射流膜乳化装置的原理及操作步骤； （3）熟练掌握乳液的表征手段； （4）了解陶瓷膜制备方法。

2. 参考文献

[1] Silvestre De Los Reyes J, Charcosset C. Preparation of water-in-oil and ethanol-in-oil emulsions by membrane emulsification[J]. Fuel, 2010,89(11):3482~3488. [2] Hancocks R D, Spyropoulos F, Norton I T. Comparisons between membranes for use in cross flow membrane emulsification[J]. Journal of Food Engineering, 2013,116(2):382~389. [3] Su#225;rez M A, Guti#233;rrez G, Matos M, et al. Emulsification using tubular metallic membranes[J]. Chemical Engineering and Processing: Process Intensification, 2014,81:24~34. [4] Matos M, Su#225;rez M A, Guti#233;rrez G, et al. Emulsification with microfiltration ceramic membranes: A different approach to droplet formation mechanism[J]. Journal of Membrane Science, 2013,444:345~358. [5] Lloyd D M, Norton I T, Spyropoulos F. Process optimisation of rotating membrane emulsification through the study of surfactant dispersions[J]. Journal of Food Engineering, 2015,166:316~324. [6] Lloyd D M, Norton I T, Spyropoulos F. Processing effects during rotating membrane emulsification[J]. Journal of Membrane Science, 2014,466:8~17. [7] Hancocks R D, Spyropoulos F, Norton I T. The effects of membrane composition and morphology on the rotating membrane emulsification technique for food grade emulsions[J]. Journal of Membrane Science, 2016,497:29~35. [8] Albert K, Vatai G, Giorno L, et al. Energy-saving potential of cross-flow membrane emulsification by ceramic tube membrane with inserted cross-section reducers [J]. Membrane Water Treatment, 2016,7(3):175~191. [9] Hornig N, Fritsching U. Membrane Emulsification of Liquid Metal for the Generation of Spherical Metal Particles[J]. Chemie Ingenieur Technik, 2014,86(3):335~340. [10] Sabouni R, Gomaa H, Liu J, et al. Emulsification Characteristics Using a Dynamic Woven Metal Microscreen Membrane[J]. Membranes, 2016,6(2):34. [11] Bux J, Manga M S, Hunter T N, et al. Manufacture of poly(methyl methacrylate) microspheres using membrane emulsification[J]. Philos Trans A Math Phys Eng Sci, 2016,374(2072). [12] Charcosset C, Limayem I, Fessi H. The membrane emulsification process#8212;a review[J]. Journal of Chemical Technology Biotechnology, 2004,79(3):209~218. [13] 景文珩, 吴俊, 邢卫红, 等. 二次膜射流乳化法制备单分散乳状液研究[J]. 化学工程, 2006(08):40~43. [14] 程昌敬, 褚良银, 陈文梅, 等. 微孔膜乳化过程中乳滴大小的控制[J]. 过滤与分离, 2005(02):4~6. [15] 穆锐, 邓爱民, 尾见信三. 用SPG膜乳化法合成单分散性高分子微粒子[J]. 高分子材料科学与工程, 2003(04):82~84. [16] Su#225;rez M A, Guti#233;rrez G, Matos M, et al. Emulsification using tubular metallic membranes[J]. Chemical Engineering and Processing: Process Intensification, 2014,81:24~34. [17] 科学实验膜乳化和微流控法制备单分散W/O乳液的研究[J]. [18] 巩方玲, 马光辉. 膜乳化技术的发展与应用: 2014年全国高分子材料科学与工程研讨会, 成都, 2014[C]. [19] 甄宗晴, 金江, 孙启梅, 等. 膜乳化法制备乳化柴油的研究[J]. 精细石油化工进展, 2008,9(3):23~26. [20] 洪波, 王保国. 膜乳化法制备微小粒径单分散乳液[J]. 清华大学学报(自然科学版), 2006(03):389~391. [21] 李娜, 陈登飞. 膜乳化过程研究进展[J]. 膜科学与技术, 2006(04):71~77. [22] 卢素敏, 王洪卫, 马友光. 膜参数对乳化过程的影响[J]. 化学工业与工程技术, 2006(02):32~37.

3. 毕业设计（论文）进程安排

2017.2-2017.3陶瓷膜的表征； 2017.3-2017.4考察不同的参数下，射流膜乳化技术制备的乳液； 2017.4-2017.5优化参数，寻求最优的操作条件； 2017.5-2017.6书写毕业论文。