中空纤维NaY分子筛膜用于甲醇/甲基叔丁基醚渗透汽化分离任务书
2020-06-24 19:47:18
1. 毕业设计(论文)的内容和要求
1、了解NaY分子筛膜在渗透汽化分离甲醇/MTBE方向的研究进展,熟悉分离原理; 2、熟悉NaY分子筛膜的制备方法; 3、考察合成液配比,合成参数(涂晶条件、合成时间、合成温度、碱度)对分子筛膜结构的影响; 4、掌握分子筛膜渗透汽化分离测试方法。
2. 参考文献
[1]陆莹. FAU沸石分子筛及其膜的合成与表征[D]. 吉林大学, 2014. [2] Kita H, Fuchida K, Horita T, et al. Preparation of faujasite membranes and their permeation properties[J]. Separation and purification technology, 2001, 25(1-3): 261-268. [3] Gu X, Dong J, Nenoff T M. Synthesis of defect-free FAU-type zeolite membranes and separation for dry and moist CO2/N2 mixtures[J]. Industrial engineering chemistry research, 2005, 44(4): 937-944. [4] Kita H, Inoue T, Asamura H, et al. NaY zeolite membrane for the pervaporation separation ofmethanol#8211;methyl tert-butyl ether mixtures[J]. Chemical Communications, 1997 (1): 45-46. [5] Kita H, Asamura H, Tanaka K, et al. Preparation and pervaporation properties of X-and Y-type zeolite membranes[M]. 2000. [6] Kusakabe K, Kuroda T, Murata A, et al. Formation of a Y-type zeolite membrane on a porous α-alumina tube for gas separation[J]. Industrial engineering chemistry research, 1997, 36(3): 649-655. [7] Zhou C, Zhou J, Huang A. Seeding-free synthesis of zeolite FAU membrane for seawater desalination by pervaporation[J]. Microporous and Mesoporous Materials, 2016, 234: 377-383. [8] Sawamura K, Furuhata T, Sekine Y, et al. Zeolite Membrane for Dehydration of Isopropylalcohol#8211;Water Mixture by Vapor Permeation[J]. ACS applied materials interfaces, 2015, 7(25): 13728-13730.
3. 毕业设计(论文)进程安排
2018.1.8~2018.3.2 查阅文献,翻译英文文章,撰写开题报告; 2018.3.3~2018.3.9 熟悉实验装置及流程; 2018.3.10~2018.4.30 实验研究,总结规律,处理实验数据; 2018.5.1~2018.6.1 撰写毕业论文,准备答辩。