水溶液中聚合诱导自组装聚酯纳米粒子的合成任务书
2020-05-02 17:10:08
1. 毕业设计(论文)的内容和要求
1. 学习并掌握聚己内酯、开环聚合和聚合物纳米粒子表征等基本概念。
2. 学习并掌握试剂提纯、聚合操作和产物表征等实验技能。
3. 学习并掌握mestrenova、origin、word、excel等化学专业和办公软件的使用方法。
2. 参考文献
[1] Hamley I W. The physics of block copolymers[M]. Oxford:Oxford Publish Press,1999:1 - 432. [2] Bates F S,Fredrickson G H. Block copolymers-designer soft materials[J]. Phys Today,1999,52(2):32-38. [3] Kataoka K,Harada A,Nagasaki Y. Block copolymer micelles for drug delivery:Design,characterization and biological signifi cance[J]. Adv Drug Del Rev,2001,47(1):113 - 131. [4] Bronstein L M,Chernyshov D M,Karlinsey R,et al. Mesoporous alumina and aluminosilica with Pd and Pt nanoparticles:Structure and catalytic properties[J]. Chem Mater,2003,15(13):2623 - 2631. [5] Zhang L F,Eisenberg A. Multiple morphologies of ”crewcut” aggregates of polystyrene-b-poly(acrylic acid) blockcopolymers[J]. Science,1995,268( 5218):1728 - 1731. [6] Thurmond K B,Kowalewski A T,Wooley K L. Watersoluble knedel-like structures:The preparation of shell-crosslinked small particles[J]. J Am Chem Soc,1996,118(30):7239 - 7240. [7] Bridgestone Corporation. Nano-particle preparation and applications:US6437050[P]. 2002 - 8 - 20. [8] Wang Xiaorong,Hall J E,Warren S Krom J,et al. Synthesis,characterization,and application of novel polymeric nanoparticles[J]. Macromolecules,2007,40 (3):499 -508. [9] Charleux B,Delaittre G,Rieger J,et al. Polymerizationinduced self-assembly:From soluble macromolecules to block copolymer nano-objects in one step[J]. Macromolecules,2012,45(17):6753 - 6765. [10] Qu Qingwu,Liu Guangyao,L#252; Xiaoqing,et al. In situ cross-linking of vesicles in polymerization-induced self-assembly[J]. ACS Macro Lett,2016,5(3):316 - 320
3. 毕业设计(论文)进程安排
2018.12.26~2018.12.30 确定课题,下达任务书,查阅文献,做好开题前期工作 2019.1.1~2019.1.18 查阅文献,做出研究方案,完成外文翻译和开题报告,开始实验 2019.2.20~2018.3.24 总结前一阶段工作,完成中期自检和中期汇报,确定下一阶段目标 2019.3.25~2019.4.30 扩展课题研究范围,改进实验方案,对 数据整理分析,撰写论文 2019.5.1~2019.6.7 完善毕业论文 2019.6.7~2019.6.14 准备毕业答辩