新型介孔Au/TiO2催化剂的合成及其催化性能的研究任务书
2020-05-18 21:18:08
1. 毕业设计(论文)的内容和要求
研究内容:合成au@tio2核壳结构。
研究方法:应用xrd、bet、fe-sem、icp、h2-tpr等表征手段研究负催化剂的结构、比表面积、孔径、形貌、金属含量等。
要求: 1. 查阅国内外相关文献,对其进行归纳总结。
2. 参考文献
[1] Kong Y, Zhang R, XU X J, et al. Synthesis and Characterization of V-MCM41 with High Vanadium Content [J]. Chinese J Inorg Chem, 2008, (24):1124-1127. [2] Council N R. Catalysis looks to the future[M]. National Academies Press, 1992. [3] Huo Q, Margolese D I, Ciesla U, et al. Organization of organic molecules with inorganic molecular species into nanocomposite biphase arrays[J]. Chem Mater, 1994, 6 [4] Chen S Y, Tang C Y, Chuang W T, et al. A facile route to synthesizing functionalized mesoporous SBA-15 materials with platelet morphology and short mesochannels[J]. Chem Mater, 2008, 20 (12): 3906-3916. [5] Huo Q, Margolese D I, Ciesla U. Generalized synthesis of periodic surfactant/inorganic composite materials[J]. Nature, 1994, 368:317-321. [6] Ciesla U, Demuth D, Leon R, et al. Surfactant controlled preparation of mesostructured transition-metal oxide compounds[J]. Chem Commun, 1994, 11: 1387-1388. [7] Bagshaw S A, Prouzet E, Pinnavaia T J. Templating of mesoporous molecular sieves by nonionic polyethylene oxide surfactants[J]. Science, 1995, 269 (5228): 1242. [8] R.B. Yu, F.S. Xiao, D. Wang, J.M. Sun, Y. Liu, G.S. Pang, S.H. Feng, S.L. Qiu, R.R. Xu, C.G. Fang, Cata. Today 51 (1999) 39-46.Ciesla U, Demuth D, Leon R, et al. Surfactant controlled preparation of mesostructured transition-metal oxide compounds[J]. Chem Commun, 1994, 11: 1387-1388. [9] Kong Y, Zhu H, Yang G, et al. Investigation of the Structure of MCM-41 Samples with a High Copper Content[J]. Adv Funct Mater, 2004, 14 (8): 816-820.
3. 毕业设计(论文)进程安排
2015-03-01#8212;03-15 查阅国内外有关文献,拟订实验方案。
2015-03-15#8212;03-20 翻译外文文献,并撰写文献综述。
2015-03-20#8212;04-10 按照拟定的实验方案依次进行实验。