1. 毕业设计（论文）的内容和要求

研究内容： 采用真空抽吸法对中空纤维DDR分子筛膜进行表面亲水层涂覆，提高膜的渗透汽化脱水分离性能。

基本要求： 1、查阅相关文献，具备英文文献阅读、整理和归纳的能力； 2、熟悉分子筛膜渗透汽化基本原理； 3、掌握实验数据处理分析能力，学会Origin制图； 4、规范书写毕业论文，认真准备答辩ppt。

2. 参考文献

[1] J. Gascon, F. Kapteijn, B. Zornoza, V. Sebastian, C. Casado, J. Coronas, Practical Approach to Zeolitic Membranes and Coatings: State of the Art, Opportunities, Barriers, and Future Perspectives, Chemistry of Materials, 2012, 24(15):2829-2844. [2] A. Malekpour, M.R. Millani, M. Kheirkhah, Synthesis and characterization of a NaA zeolite membrane and its applications for desalination of radioactive solutions, Desalination, 2008, 225:199-208. [3] K. Sato, K. Aoki, K. Sugimoto, K. Izumi, S. Inoue, J. Saito, S. Ikeda, T. Nakane, Dehydrating performance of commercial LTA zeolite membranes and application to fuel grade bio-ethanol production by hybrid distillation/vapor permeation process, Microporous and Mesoporous Materials, 2008, 115:184-188. [4] K. Sato, T. Nakane, A high reproducible fabrication method for industrial production of high flux NaA zeolite membrane, Journal of Membrane Science, 2007, 301:151-161. [5] K. Sato, K. Sugimoto, T. Nakane, Preparation of higher flux NaA zeolite membrane on asymmetric porous support and permeation behavior at higher temperatures up to 145 #176;C in vapor permeation, Journal of Membrane Science, 2008, 307:181-195. [6] V. Van Hoof, C. Dotremont, A. Buekenhoudt, Performance of Mitsui NaA type zeolite membranes for the dehydration of organic solvents in comparison with commercial polymeric pervaporation membranes, Separation and Purification Technology, 2006, 48:304-309. [7] C.H. Cho, K.Y. Oha, J.G. Yeo, S.K. Kima, Y.M. Lee, Synthesis, ethanol dehydration and thermal stability of NaA zeolite/alumina composite membranes with narrow non-zeolitic pores and thin intermediate layer, Journal of Membrane Science, 2010, 364:138-148. [8] A. Huang, W. Yang, J. Liu, Synthesis and pervaporation properties of NaA zeolite membranes prepared with vacuum-assisted method, Separation and Purification Technology, 2007, 56:158-167. [9] V.V. Namboodiri, L.M. Vane, High permeability membranes for the dehydration of low water content ethanol by pervaporation, Journal of Membrane Science, 2007, 306:209-215. [10] T.C. Bowen, R.D. Noble, J.L. Falconer, Fundamentals and applications of pervaporation through zeolite membranes, Journal of Membrane Science, 2004, 245:1#8211;33. [11] J. Caro, M. Noack, P. Kolsch, Zeolite membranes from the laboratory scale to technical applications. Adsorption, 2005, 11(3): 215-227. [12] J. van den Bergh, W. Zhu, J. Gascon, J.A. Moulijn, F. Kapteijn, Separation and permeation characteristics of a DD3R zeolite membrane, Journal of Membrane Science, 2008, 316:35-45. [13] J. Zhang, M. Li, Y. Lin, C. Liu, X. Liu, L. Bai, D. Hu, G. Zeng, Y. Zhang, W. Wei, Y. Sun, Synthesis and characterization of all-silica DDR zeolite by microwave heating, 2016, 219, 103-111. [14] T. Tomita, K. Nakayama, H. Sakai, Gas separation characteristics of DDR type zeolite membrane, Microporous and Mesoporous Materials, 2004, 68:71-75. [15] F. Zheng, W. Jing, X. Gu, N. Xu, J. Dong, Rapid synthesis of pure DD3R zeolite using ball-milled Sigma-1 seeds under static conditions, Journal of Material Science, 2013, 48:6286-6292. [16] S. Yang, Z. Cao, A. Arvanitis, X. Sun, Z. Xu, J. Dong, DDR-type zeolite membrane synthesis, modification and gas permeation studies, Journal of Membrane Science, 2016, 505:194-204. [17] J. Kuhn, J. Gascon, J. Gross, F. Kapteijn, Detemplation of DDR type zeolites by ozonication, Microporous and Mesoporous Materials, 2009, 120:12-18. [18] A. Bose, J. Kishore Das, N. Das, Pore modification of deca-dodecasil-rhombohedral zeolite membrane by carbon loading from in situ decomposition of 1-adamantanamine for improved gas separation, RSC Advances, 2015, 5:67195-67205. [19] J. Kuhn, J. Castillo-Sanchez, J. Gascon, S. Calero, D. Dubbeldam, T. Vlgut, F. Kapteijn, J. Gross, Adsorption and diffusion of water, methanol, and ethanol in all-silica DD3R: Experiments and simulation. Journal of Physical Chemistry C, 2009, 113:14290-14301.

3. 毕业设计（论文）进程安排

2月-3月 阅读相关文献，完成外文翻译，文献综述等； 3月-5月 亲水性DDR分子筛膜的制备、表征与渗透汽化分离测试； 5月-6月 撰写本科毕业论文、答辩。