缩孔Fe-SBA-15的制备及其苯酚羟基化性能任务书
2020-06-10 22:07:23
1. 毕业设计(论文)的内容和要求
通过一步合成法合成缩孔fe-sba-15。
主要是调和ctab和p123两种表面活性剂的比例来达到调节孔径的目的,并研究ph及铁含量对催化剂的影响。
并对制备的催化剂进行催化性能的检测。
2. 参考文献
1 R. A. Sheldon and J. K. Kochi, Metal Catalyzed Oxidations of Organic Compounds, Academic Press, New York, 1981. 2 R. Alcantara, L. Canoira, P. G. Joao, J. M. Santos and I. Va′zquez, Appl. Catal., A, 2000, 203, 259#8211;268. 3 A. Corma, Chem. Rev., 1997, 97, 2373#8211;2419. 4 R. Chakravarti, P. Kalita, S. T. Selvan, H. Oveisi, V. V. Balasubramanian, M. L. Kantam and A. Vinu, Green Chem., 2010, 12, 49#8211;53. 5 Z. Luan, M. Hatmann, D. Zhao, W. Zhou and L. Kevan, Chem. Mater., 1999, 11, 1621#8211;1627. 6 R. M. Mart#305;′n-Aranda and J. Cejka, Top. Catal., 2010, 53,141#8211;153. 7 K. Ariga, A. Vinu, Y. Yamauchi, Q. Ji and J. P. Hill, Bull. Chem. Soc. Jpn., 2012, 85, 1#8211;32. 8 M. Claudia Marchi, J. J. S. Acuna and C. A. Figueroa, J. Nanosci. Nanotechnol., 2012, 12, 6439#8211;6444. 9 M. B. Zakaria, N. Suzuki, K. Shimasaki, N. Miyamoto,Y. T. Huang and Y. Yamauchi, J. Nanosci. Nanotechnol.,2012, 12, 4502#8211;4507. 10 W. Xuan, C. Zho, Y. Liu and Y. Cui, Chem. Soc. Rev., 2012,41, 2590#8211;2604. 11 Z. Li, J. C. Barnes, A. Bosoy, J. F. Stoddart and J. I. Zink,Chem. Soc. Rev., 2012, 41, 1677#8211;1693. 12 D. Zhao, J. Feng, Q. Huo, N. Melosh, G. Fredrikson, B. F. Chemelka and G. D. Stucky, Science, 1998, 279,548#8211;552. 13 R. Ryoo, J. M. Kim, C. H. ko and C. H. Shin, J. Phys. Chem., 1996, 100, 17718#8211;17721. 14 R. R. Murugavel and H. W. Roesky, Angew. Chem., 1997, 109, 491#8211;494. 15 A. Vinu, V. Murugesan and M. Hartmann, Chem. Mater., 2003, 15, 1385#8211;1393.
3. 毕业设计(论文)进程安排
2017-02-24#8212;03-10 查阅国内外有关文献,拟订实验方案。
2017-03-10#8212;03-20 翻译外文文献,并撰写文献综述。
2017-03-20#8212;04-10 按照拟定的实验方案依次进行实验。