1. 毕业设计（论文）的内容和要求

在查阅文献的基础上，合成纳米尺度的铂铁催化剂，并使用xrd、sem等分析技术，表征获得产品的各项参数。

在进行毕业设计的过程中，培养阅读中外文献资料以及独立开展实验研究、独立思考和分析问题解决问题的能力。

锻炼各类科学绘图工具以及数据处理软件的实用，学习并熟练操作电化学测试常用的技术和实验方法，并最终高质量的完成毕业论文的撰写。

2. 参考文献

1. Steele, B. C. H., Heinzel, A. Materials for fuel-cell technologies. Nature 414, 345-352 (2001). 2. Debe, M. K. Electrocatalyst approaches and challenges for automotive fuel cells. Nature 486, 43-51 (2012). 3. Duan, H. M., Xu, C. X. Nanoporous PtPd Alloy Electrocatalysts with High Activity and Stability toward Oxygen Reduction Reaction. Electrochim. Acta 152, 417-424 (2015). 4. Al-Akraa, I. M., Mohammad, A. M., El-Deab, M. S., El-Anadouli, B. E. Electrocatalysis by design: Synergistic catalytic enhancement of formic acid electro-oxidation at core-shell Pd/Pt nanocatalysts. Int. J. Hydrogen Energy 40, 1789-1794 (2015). 5. Dang, D., Liao, S. J., Luo, F., Hou, S. Y., Song, H. Y., Huang, P. Y. A pulse electrochemical deposition method to prepare membrane electrode assemblies with ultra-low anode Pt loadings through in situ construction of active core-shell nanoparticles on an electrode. J. Power Sources 260, 27-33 (2014). 6. Cochell, T., Li, W., Manthiram, A. Effects of Pt Coverage in Pt@PdCu5/C Core-Shell Electrocatalysts on the Oxygen Reduction Reaction and Methanol Tolerance. J. Phys. Chem. C 117, 3865-3873 (2013). 7. Ferreira, E. H. M., Moutinho, M. V. O., Stavale, F., Lucchese, M. M., Capaz, R. B., Achete, C. A., Jorio, A. Evolution of the Raman spectra from single-, few-, and many-layer graphene with increasing disorder. Phys. Rev. B 82, (2010). 8. Cancado, L. G., Jorio, A., Ferreira, E. H. M., Stavale, F., Achete, C. A., Capaz, R. B., Moutinho, M. V. O., Lombardo, A., Kulmala, T. S., Ferrari, A. C. Quantifying Defects in Graphene via Raman Spectroscopy at Different Excitation Energies. Nano Lett. 11, 3190-3196 (2011). 9. Kim, J., Lee, Y., Sun, S. H. Structurally Ordered FePt Nanoparticles and Their Enhanced Catalysis for Oxygen Reduction Reaction. J. Am. Chem. Soc. 132, 4996- (2010).

3. 毕业设计（论文）进程安排

2018年3月 阅读文献和熟悉实验室所有仪器设备。

2018年4月-5月 进行铂铁催化剂的合成，得到最优化的产品合成参数。

2018年6月 进行催化剂的表征和电化学性能测试，并在此基础上撰写毕业论文。