1. 毕业设计（论文）的内容和要求

1、学会常用数据库的使用，熟练掌握中外文文献的搜集 2、通过对文献的总结了解负载型催化剂的常规制备方法，表征手段。

3、熟悉相关实验仪器的具体使用方法，熟悉正确安全的实验步骤 4、通过撰写论文，加深对专业科目的了解，并扩展自己的知识领域

2. 参考文献

参考文献 [1] Lambert A, Macquarrie D J, Carr G, et al. The catalytic oxidation of cyclohexanone to caprolactone using hexagonal mesoporous silica supported SbF3[J]. NEW J. CHEM. 2000, 24(7): 485~488. [2] Marczewski M, Marczewska H, Witoslawski K. SUPERACID PROPERTIES OF AL2O3-SBF5 CATALYTIC-SYSTEM[J]. J. MOL. CATAL. A-CHEM. 1995, 97(2): 101~110. [3] Tang L, Li B, Zhai Z, et al. Selective oxidation of diphenylmethane over cobalt doped mesoporous titania-silica catalyst with high Ti content[J]. CATAL. LETT. 2008, 121(1-2): 63~69. [4] Maleki B, Mofrad A V, Khojastehnezhad A. SbCl3-SiO(2)AS AN EFFICIENT AND HETEROGENEOUS CATALYST FOR THE SYNTHESIS OF POLYHYDROQUINOLINE DERIVATIVES UNDER SOLVENT-FREE CONDITIONS[J]. HETEROCYCLIC LETTERS. 2017, 7(1): 17~25. [5] Massa M, Andersson A, Finocchio E, et al. Performance of ZrO2-supported Nb- and W-oxide in the gas-phase dehydration of glycerol to acrolein[J]. J. CATAL. 2013, 297: 93~109. [6] Shiju N R, Brown D R, Wilson K, et al. Glycerol Valorization: Dehydration to Acrolein Over Silica-Supported Niobia Catalysts[J]. TOP. CATAL. 2010, 53(15-18): 1217~1223. [7] Safari J, Gandomi-Ravandi S, Naseh S. Efficient, green and solvent-free synthesis of tetrasubstituted imidazoles using SbCl3/SiO2 as heterogeneous catalyst[J]. J. CHEM. SCI. 2013, 125(4): 827~833. [8] Clark J H, Macquarrie D J. Catalysis of liquid phase organic reactions using chemically modified mesoporous inorganic solids[J]. CHEM. COMMUN. 1998(8): 853~860. [9] Kapoor K K, Ganai B A, Kumar S, et al. Antimony(III) chloride impregnated on alumina - An efficient and economical Lewis acid catalyst for one-pot synthesis of dihydropyrimidinones under solvent-free conditions[J]. CANADIAN JOURNAL OF CHEMISTRY-REVUE CANADIENNE DE CHIMIE. 2006, 84(3): 433~437. [10] Zhang Z, Liu Y. Antimony trichloride/SiO(2) promoted synthesis of 9-ary-3,4,5,6,7,9-hexahydroxanthene-1,8-diones[J]. CATAL. COMMUN. 2008, 9(8): 1715~1719. [11] Yoshikawa N, Doyle A, Tan L, et al. An efficient and scalable synthesis of substituted phenanthrenequinones by intramolecular friedel-crafts reaction of imidazolides[J]. ORG. LETT. 2007, 9(21): 4103~4106.

3. 毕业设计（论文）进程安排

2018.02.26-2018.03.10 查阅国内外有关文献，做文献综述；完成外文翻译；拟定实验方案。

2018.03.10-2018.05.10 按照实验要求进行各种实验工作。

2018.05.10-2018.06.01 进行实验数据的处理，补充有关实验，开始撰写论文。