含氟改性聚乙烯亚胺材料的制膜工艺研究任务书
2020-04-21 16:58:33
1. 毕业设计(论文)的内容和要求
1.掌握文献检索的方法和技巧,了解有机纳滤膜材料的制备方法; 重点掌握界面聚合工艺,具体表现在熟悉界面聚合操作流程,研究该工艺中关键要素对成膜性能的影响。
2.熟悉科研过程,培养独立思考问题的能力,锻炼实验能力,尝试解决科研中的问题。
3.掌握膜材料的相关表征手段及膜应用性能的测试方法。
2. 参考文献
[1]Feng C , Xu J , Li M , et al. Studies on a novel nanofiltration membrane prepared by cross-linking of polyethyleneimine on polyacrylonitrile substrate[J]. Journal of Membrane Science, 2014, 451:103-110; [2]Wei X , Hong J , Zhu S , et al. Structure#8211;performance study of polyamide composite nanofiltration membranes prepared with polyethyleneimine[J]. Journal of Materials Science, 2017, 52(19):11701-11714; [3]Raaijmakers M J T , Benes N E . Current trends in interfacial polymerization chemistry[J]. Progress in Polymer Science, 2016,63:86-142; [4]邢卫红, 顾学红. 高性能膜材料与膜技术[M]. 北京:化学工业出版社,2017; [5]Wu D , Huang Y , Yu S , et al. Thin film composite nanofiltration membranes assembled layer-by-layer via interfacial polymerization from polyethylenimine and trimesoyl chloride[J]. Journal of Membrane Science, 2014, 472:141-153; [6]Lv Y , Yang H C , Liang H Q , et al. Nanofiltration membranes via co-deposition of polydopamine/polyethylenimine followed by cross-linking[J]. Journal of Membrane Science, 2015, 476:50-58; [7]Klaysom C , Hermans S , Gahlaut A , et al. Polyamide/Polyacrylonitrile (PA/PAN) thin film composite osmosis membranes: Film optimization, characterization and performance evaluation[J]. Journal of Membrane Science, 2013, 445:25-33; [8]Lai G S , Lau W J , Goh P S , et al. Tailor-made Thin Film Nanocomposite Membrane Incorporated with Graphene Oxide using Novel Interfacial Polymerization Technique for Enhanced Water Separation[J]. Chemical Engineering Journal, 2018,344:524-534; [9]Shan L , Gu J , Fan H , et al. Micro-phase diffusion-controlled interfacial polymerization for an ultrahigh permeability nanofiltration membrane[J]. ACS Applied Materials Interfaces, 2017,9:44820-44827; [10]S. P. Sun, T. A. Hatton, T. S. Chung, Environ. Sci. Technol. 2011, 45: 4003-4009.
3. 毕业设计(论文)进程安排
2018/2/22 - 2018/3/10:文献检索,做好实验设计,确定实验方法。
2018/3/11 - 2018/4/20:以聚乙烯亚胺为原料,制备一批膜材料,并对其性能进行考察,筛选其最优制膜条件; 2018/4/21 - 2018/5/31:以含氟改性聚乙烯亚胺为原料,制备一批膜材料,并对其性能进行考察,筛选其最优制膜条件; 2018/6/1 - 2018/6/10:关联两类膜材料数据,分析数据,撰写论文。