1. 毕业设计（论文）的内容和要求

主要是石墨烯/氧化镍纳米复合纤维的制备及其柔性超级电容器的应用研究学习。

要求学生能独立运用数据处理软件，并具有初步的实验数据分析能力，利用word撰写论文，PowerPoint制作答辩报告。

2. 参考文献

三．应收集的资料及主要参考文献 [1] Liyang Lin, Tianmo Liu, Jianlin Liu, Kemeng Ji, Rong Sun,bWen Zeng and Zhongchang Wang.Synthesis of carbon fiber@nickel oxide nanosheet core#8211;shells for high-performance supercapacitors [J], The Royal Society of Chemistry, 2015, 5, 84238#8211;84244 . [2] Xingjiang Wu, Yijun Xu, Ying Hu, Guan Wu , Hengyang Cheng, Qiang Yu, Kai Zhang,Wei Chen Su Chen. Microfluidic-spinning construction of blackphosphorus- hybrid microfibres for non-woven fabrics toward a high energy density flexible supercapacitor [J]. NATURE COMMUNICATIONS.2018,10.1038/s41467-018-06914-7. [3] Yu-Long Tong, Bin Xu, Xia-Fang Du, Heng-Yang Cheng, Cai-Feng Wang, Guan Wu,and Su Chen. Microfluidic-Spinning-Directed Conductive Fibers toward Flexible Micro-Supercapacitors [J].MACROMOLECULAR MATERIAS AND ENGINEERING,2018, 1700664. [4] Qing Li,Hengyang Cheng, Xingjiang Wu, Cai-Feng Wang, Guan Wu and Su Chen. Enriched carbon dots/graphene microfibers towards high-performance micro-supercapacitors [J].The Royal Society of Chemistry , 2018, 6,14112. [5] Xingjiang Wu,Guan Wu, Pengfeng Tan, Hengyang Cheng, Ri Hong, Fengxiang Wang and Su Chen. Construction of microfluidic-oriented polyaniline nanorod arrays/graphene composite fibers for application in wearable micro-supercapacitors [A]. The Royal Society of Chemistry ,2018, 6,8940. [6] Guan Wu, Pengfeng Tan, Xingjiang Wu, Lu Peng, Hengyang Cheng, Cai-Feng Wang,Wei Chen, Ziyi Yu, and Su Chen. High-Performance Wearable Micro-Supercapacitors Based on Microfluidic-Directed Nitrogen-Doped Graphene Fiber Electrodes.ADVANCED FUNNCTIONAL MATERIALS, 2017, 27, 1702493. [7] Zhuoxin Liu, Funian Mo, Hongfei Li, Minshen Zhu, Zifeng Wang, Guojin Liang,and Chunyi Zhi. Advances in Flexible and Wearable Energy-Storage Textiles.Small Methods, 2018, 1800124. [8] Liang Huang, Diana Santiago, Patricia Loyselle, and Liming Dai. Graphene-Based Nanomaterials for Flexible and Wearable Supercapacitors.Nano Micro Small. 2018, 1800879. [9] Guofeng Zhang, Yuyang Han, Changxiang Shao, Nan Chen, Guoqiang Sun,Xuting Jin, Jian Gao, Bingxue Ji, Hongsheng Yang and Liangti Qu. Processing and manufacturing of graphene-based microsupercapacitors. The Royal Society of Chemistry and the Chinese Chemical Society. 2018,10.1039/c8qm00270c [10] Qiuyan Yang, Zhen Xu, Chao Gao. Graphene fiber based supercapacitors: Strategies and perspective toward high performances. Journal of Energy Chemistry,2018(27) :6#8211;11. [11]Changzhou Yuan, Xiaogang Zhang,Linhao Su, Bo Gao and Laifa Shen. Facile synthesis and self-assembly of hierarchical porous NiO nano/micro spherical superstructures for high performance supercapacitors. Journal of Materials Chemistry,2009, 10.1039/b902221j. [12] Zhen Xu and Chao Gao. Graphene in Macroscopic Order: Liquid Crystals and Wet-Spun Fibers. Accounts of Chemical Research, 2014, 47, 1267#8722;1276. [13] Wang J, Yang M, Zheng Z J, et al. Design, preparation and assembly of flexible electrode based on carbon materials (in Chinese). Chin Sci Bull,2019, 64: 514#8211;531, doi: 10.1360/N972018-01105.

3. 毕业设计（论文）进程安排

2019 . 2 . 21 ~ 2019 . 3. 10 ：了解课题背景，资料收集整理，阅读有关文献，完成开题报告； 2019 .3 . 11 ~ 2019 . 4 .11：利用天然石墨粉制备氧化石墨烯，通过热组装方法制备石墨烯纤维；在纤维表面生长氧化镍纳米阵列； 2019 . 4 . 12 ~ 2019. 5 . 12 ：对制备的石墨烯/氧化镍复合纤维进行电化学表征以及形貌表征，并处理实验数据； 2019 . 5 . 13 ~ 2019 . 6 . 10 ：总结实验结果，对所得的测试结果进行分析，完成毕业论文，准备论文答辩。