1. 毕业设计（论文）的内容和要求

1. 学会用各种文献检索手段对课题进行检索； 2.培养独立开展实验研究、独立思考的能力； 3.培养综合运用所学专业知识分析、解决实际问题的能力； 4.培养实验方案的制定、仪器设备的选型、安装、调试及实验数据的测试、采集与分析处理的能力； 5.科技论文的写作能力。

2. 参考文献

[1] 王艳红, 何小波, 银凤翔,等. 电催化氧气析出贵金属催化剂的研究进展[J]. 新型工业化, 2016, 6(12):1-8. [2] 胡玮. 铱基氧析出催化剂的制备与电化学性质研究[D]. 武汉大学, 2012. [3] 唐致远, 宋世栋, 刘建华. 钙钛矿型双功能氧电极催化剂的研究进展[J]. 电源技术, 2003, 27(b05):233-237. [4] 杨洋,马雨蒙,李朋伟,李巧霞.非贵金属氧还原电催化剂的研究进展[J].电池,2018,48(01):56-59. [5] D. Chen, C. Chen, Z. M. Baiyee, Z. Shao, F. Ciucci, Nonstoichiometric oxides as low-cost and highly-efficient oxygen reduction/evolution catalysts for low-temperature electrochemical devices. Chem. Rev. 115, 9869#8211;9921 (2015). [6] Z. Shao, W. Zhou, Z. Zhu, Advanced synthesis of materials for intermediate-temperature solid oxide fuel cells. Prog. Mater. Sci. 57, 804#8211;874 (2012). [7] Y. Zhu, W. Zhou, Z.-G. Chen, Y. Chen, C. Su, M. O. Tad#233;, Z. Shao, SrNb0.1Co0.7Fe0.2O3-d perovskite as a next-generation electrocatalyst for oxygen evolution in alkaline solution.Angew. Chem. Int. Ed. 54, 3897#8211;3901 (2015). [8] Y. Matsumoto, E. Sato, Electrocatalytic properties of transition metal oxides for oxygen evolution reaction. Mater. Chem. Phys. 14, 397#8211;426 (1986). [9] B. Zhang, X. Zheng, O. Voznyy, R. Comin, M. Bajdich, M. Garc#237;a-Melchor, L. Han, J. Xu,M. Liu, L. Zheng, F. P. Garc#237;a de Arquer, C. T. Dinh, F. Fan, M. Yuan, E. Yassitepe, N. Chen,T. Regier, P. Liu, Y. Li, P. De Luna, A. Janmohamed, H. L. Xin, H. Yang, A. Vojvodic,E. H. Sargent, Homogeneously dispersed multimetal oxygen-evolving catalysts. Science352, 333#8211;337 (2016). [10] a) T. P. Cook, D. K. Dogutan, S. Y. Reece, Y. Surendranath,T. S. Teets, D. G. Nocera, Chem. Rev. 2010, 110, 6474; b) S. Dou,L. Tao, R. Wang, S. E. Hankari, R. Chen, S. Wang, Adv. Mater. 2018,30, 1705850 [11] a) Y. Zheng, Y. Jiao, Y. Zhu, L. H. Li, Y. Han, Y. Chen, M. Jaroniec,S. Z. Qiao, J. Am. Chem. Soc. 2016, 138, 16174; b) S. Cherevko,S. Geiger, O. Kasian, N. Kulyk, J. P. Grote, A. Savan, B. R. Shrestha,S. Merzlikin, B. Breitbach, A. Ludwig, K. J. J. Mayrhofer, Catal. Today 2016, 262, 170. [12] a) Y. Zhao, R. Nakamura, K. Kamiya, S. Nakanishi, K. Hashimoto,Nat. Commun. 2013, 4, 2390; b) Z. Liu, Z. Zhao, Y. Wang, S. Dou,D. Yan, D. Liu, Z. Xia, S. Wang, Adv. Mater. 2017, 29, 1606207; c) D. Liu,L. Tao, D. Yan, Y. Zou, S. Wang, ChemElectroChem 2018, 5, 1775. [13] a) J. Hwang, R. R. Rao, L. Giordano, Y. Katayama, Y. Yu,Y. Shao-Horn, Science 2017, 358, 751; b) B. Hua, M. Li, Y.-Q. Zhang,Y.-F. Sun, J.-L. Luo, Adv. Energy Mater. 2017, 7, 1700666; c) X. Xu,W. Wang, W. Zhou, Z. Shao, Small Methods 2018, 2, 1800071. [14] a) J. H. Myung, D. Neagu, D. N. Miller, J. T. S. Irvine, Nature2016, 537, 528; b) K. Zhu, T. Wu, M. Li, R. Lu, X. Zhu, W. Yang,J. Mater. Chem. A 2017, 5, 19836; c) Y. Zhu, J. Dai, W. Zhou,Y. Zhong, H. Wang, Z. Shao, J. Mater. Chem. A 2018, 6, 13582. [15] Z. Zeng, K.-C. Chang, J. Kubal, N. M. Markovic, J. Greeley,Nat. Energy 2017, 2, 17070 [16] P. D. Luna, R. Quintero-Bermudez, C.-T. Dinh, M. B. Ross,O. S. Bushuyev, P. Todorovi#263;, T. Regier, S. O. Kelley, P. Yang,E. H. Sargent, Nat. Catal. 2018, 1, 103. [17] M. S. Burke, M. G. Kast, L. Trotochaud, A. M. Smith,S. W. Boettcher, J. Am. Chem. Soc. 2015, 137, 3638.

3. 毕业设计（论文）进程安排

1．1-4周：阅读相关文献，了解专业背景，完成翻译。

2．5-8周：熟悉实验室的仪器设备，掌握基本的制备过程#8212;#8212;粉体的合成、磁控溅射靶材的烧制以及磁控溅射全流程的操作。

3．9-12周：采用xrd、sem等对粉体进行表征，测试粉体的结构；使用磁控溅射装置进行双靶镀膜，制得催化剂。