1. 毕业设计（论文）的内容和要求

研究内容： 以国产四乙基氢氧化铵（TEAOH）为模板剂制备SAPO-34分子筛，并通过二次生长法在四通道中空纤维载体表面制备出SAPO-34分子筛膜，用于H2/CH4体系分离。

基本要求： 1、查阅相关文献，具备英文文献阅读、整理和归纳的能力； 2、熟悉分子筛及分子筛膜制备过程； 3、了解气体分离原理及色谱操作过程； 4、掌握实验数据处理分析能力，学会Origin制图； 5、规范书写毕业论文，认真准备答辩ppt。

2. 参考文献

1. Poshusta J C, Tuan V A, Falconer A J, et al. Synthesis and permeation properties of SAPO-34 tubular membranes[J]. Industrial Engineering Chemistry Research, 1998, 37(10): 3924-3929. 2. Poshusta J C, Tuan V A, Pape E A, et al. Separation of light gas mixtures using SAPO‐34 membranes[J]. Aiche Journal, 2000, 46(4): 779-789. 3. Hong M, Falconer J L, Noble R D, et al. Modification of Zeolite Membranes for H2 Separation by Catalytic Cracking of Methyldiethoxysilane[J]. Industrial Engineering Chemistry Research, 2005, 44(11): 4035-4041. 4. Li S, Falconer J L, Noble R D, et al. Interpreting Unary, Binary, and Ternary Mixture Permeation Across a SAPO-34 Membrane with Loading-Dependent Maxwell#8722;Stefan Diffusivities[J]. Journal of Physical Chemistry C, 2007, 111(13): 5075-5082. 5. Hong M, Li S, Funke H F, et al. Ion-exchanged SAPO-34 membranes for light gas separations[J]. Microporous and Mesoporous Materials, 2007, 106(1): 140-146. 6. Hong M, Li S, Falconer J L, et al. Hydrogen purification using a SAPO-34 membrane[J]. Journal of Membrane Science, 2008, 307(2): 277-283. 7. Karatay E, Kalipcilar H, Yilmaz L, et al. Preparation and performance assessment of binary and ternary PES-SAPO 34-HMA based gas separation membranes[J]. Journal of Membrane Science, 2010, 364(1): 75-81. 8. Li G, Yang J, Wang J, et al. Thin carbon/SAPO-34 microporous composite membranes for gas separation[J]. Journal of Membrane Science, 2011, 374(1): 83-92. 9. Jabbari Z, Fatemi S, Davoodpour M, et al. Comparative study of seeding methods; dip-coating, rubbing and EPD, in SAPO-34 thin film fabrication[J]. Advanced Powder Technology, 2014, 25(1): 321-330. 10. Zhou L, Yang J, Li G, et al. Highly H2 permeable SAPO-34 membranes by steam-assisted conversion seeding[J]. International Journal of Hydrogen Energy, 2014, 39(27): 14949-14954.

3. 毕业设计（论文）进程安排

毕业论文进程安排： 2月-3月 阅读相关文献，完成外文翻译，文献综述等； 3月-5月 考察合成条件对膜形貌和结构的影响；考察操作参数对分子筛膜性能的影响 5月-6月 撰写本科毕业论文、答辩。