ZIF-8晶体合成及聚晶膜研究任务书
2020-05-19 21:26:10
1. 毕业设计(论文)的内容和要求
1、查阅有关不同形貌zif-8晶体合成方法及zif-8膜制备研究的相关文献,弄清楚课题的研究目的和意义,掌握课题的研究重点,筛选出与本课题相关性高的文献。
同时阅读课题的相关外文文献,进行总结归纳,并设计实验方案,制定实验计划。
2、熟悉实验仪器的正确使用,提高实验操作技能,合理规划实验进程。
2. 参考文献
[1] Yichang Pan, Dodi Heryadi, Feng Zhou, Lan Zhao, Gabriella Lestari, Haibin Sub and Zhiping Lai,Tuning the crystal morphology and size of zeolitic imidazolate framework-8 in aqueous solution by surfactants [J]. CrystEngComm, 2011, 13, 6937. [2]Mohammad Yaser Masoomi, Saeideh Beheshti, and Ali Morsali, Shape Control of Zn(II) Metal#8722;Organic Frameworks by Modulation Synthesis and Their Morphology-Dependent Catalytic Performance[J].Cryst. Growth Des. 2015, 15, 2533#8722;2538. [3] Hee Jung Lee, Junghun We, Jun Oh Kim, Dooyoung Kim, Wonhee Cha, Eunji Lee,Jeungwon Sohn, and Moonhyun Oh, Morphological and Structural Evolutions of Metal#8211;Organic Framework Particles from Amorphous Spheres to CrystallineHexagonal Rods[J].Angew. Chem. Int. Ed. 2015, 54, 10564 #8211;10568. [4] Yichang Pan, Yunyang Liu, Gaofeng Zeng, Lan Zhao and Zhiping Lai, Rapid synthesis of zeolitic imidazolate framework-8 (ZIF-8) nanocrystals in an aqueous system[J].Chem. Commun., 2011, 47, 2071#8211;2073. [5] Shunsuke Tanaka a,b,n, TomokoShimada a, KosukeFujita a, YoshikazuMiyake a,b, KojiKida c, Katsunori Yogo c, JoeriF.M.Denayer d, MikiSugita e, TakahikoTakewaki , Seeding-free aqueous synthesis of zeolitic imidazolate framework-8 membranes: How to trigger preferential heterogeneous nucleation and membrane growth in aqueous rapid reaction solution [J]. Journal ofMembraneScience472(2014)29#8211;38.
3. 毕业设计(论文)进程安排
2.22-3.10 查阅文献,进行相关文献的翻译工作,完成开题报告。
3.11-3.31 了解并掌握zif-8晶体的制备方法。
4.1-4.21 考察制备不同条件对zif-8晶体形貌控制的研究,并熟悉zif-8膜的合成过程。