石墨烯/ZIF-8复合材料负载钴基催化剂的制备及性能研究任务书
2020-05-19 21:28:51
1. 毕业设计(论文)的内容和要求
1)查阅、整理文献资料,加深对自己课题的理解,并撰写开题报告及文献综述。
2)要求学生对工业催化、无机材料制备基础、波谱分析等学科复习,从而对以后催化剂活性测试实验、谱图分析打下基础。
3)主要研究胶体晶体的制备以及水滑石基催化剂的制备,综合其余一些表活剂掺杂催化剂形貌结构以及催化活性的影响。
2. 参考文献
[1] 段雪,张法智.插层组装与功能材料.化学工业出版社,北京,2007. [2] B. Mavis, M. Akinc. Three-component layer double hydroxides by urea precipitation:structural stability and electrochemistry. J. Power Sources, 2004, 134: 308-317P. [3] Y. Zhao,F. Li,R. Zhang,et al. Preparation of layered double-hydroxide nanomaterials with a uniform crystallite size using a new method involving Separate nucleation and aging steps. Chem. Mater., 2002, 14(10): 4286-4291P. [4] 赵芸,矫庆泽,李峰等.非平衡晶化控制水滑石晶粒尺寸.无机化学学报,2001,17(6):830-834 页 [5] K. Chibwe, W. Jones. Intercalation of organic and inorganic anions into layered double hydroxides. J. Chem. Soc. Chem. Commun., 1989, 14: 926-927P. [6] 廖凯波.水滑石类固体碱催化剂制备及其性能研究.湘潭大学硕士学位论文.2009. [7] L. L. Qin, S. L. Wang, R. Zhang, et al. Two different approaches to synthesizing Mg-Al-layered double hydroxides as folic acid carriers. J. Phys. Chem. Solids, 2008, 69:2779-2784P. [8] F. P. Jiao, X.Q. Chen, Z.D. Fu, et al. Intercalation of Mg-Al layered double hydroxides by ( )-dibenzoyl-D-tartaric acid:Preparation and characterization. J. Mol. Struct., 2009,921:328-332P. [9] G. J. Cui, D. G. Evans, D. Q. Li. Synthesis and UV absorption properties of 5, 5-thiodisalicylic acid intercalated Zn-Al layered double hydroxides. Polym. Degrad.Stab., 2010, 95: 2082-2087P. [10] Y. F. Zhao, S. He, M. Wei, et al. Hierarchical films of layered double hydroxides by using a sol-gel process and their high adaptability in water treatment. Chem. Commun., 2010,46: 3031-3033P. [11] N. Yamaguchi, T. Nakamura, K. Tadanaga, et al. Direct Formation of Zn-Al Layered Double Hydroxide Films with High Transparency on Glass Substrate by the Sol-Gel Process with Hot Water Treatment. Cryst. Growth Des., 2006, 7: 1726-1729P. [12] F. Prinetto, G.. Ghiotti, P. Graffin, et al. Synthesis and characterization of sol-gel Mg/Al and Ni/Al layered double hydroxides and comparison with co-precipitated samples.Microporous Mesoporous Mater., 2000, 39: 229-247P. [13] J.S.Valente, M.S.Cantu, R.Montiel, et al. Preparation and Characterization of Sol GelMgAl Hydrotalcites with Nanocapsular Morphology. J. Phys. Chem. C 2007, 111: 642-651P. [14] S. He, Y. F. Zhao, M. Wei, et al. Preparation of Oriented Layered Double Hydroxide Film Using Electrophoretic Deposition and Its Application in Water Treatment. Ind. Eng.Chem. Res. 2011, 50: 2800-2806P. [15] X. Duan, D. P. Yan, J. Lu, et al. In Situ Polymerization of the 4-Vinylbenzenesulfonic Anion in Ni-Al-Layered Double Hydroxide and Its Molecular Dynamic Simulation. J.Phys. Chem. A., 2008, 112: 7671-7681P. [16] X. Duan, J. T. Feng, Y. J. Lin, et al. Enhanced metal dispersion and hydrodechlorination properties of a Ni/Al2O3 catalyst derived from layered double hydroxides. J. Catal., 2009,266: 351-358P. [17] X. Duan, X. X. Guo, S. L. Xu, et al. One-Step Hydrothermal Crystallization of a Layered Double Hydroxide/Alumina Bilayer Film on Aluminum and Its Corrosion Resistance Properties. Langmuir, 2009, 25(17): 9894-9897P.
3. 毕业设计(论文)进程安排
2016年3月10日前完成毕设系统中学生毕业设计(论文)选题、中英文翻译、任务书下达以及开题报告工作 2016年3月10日-6月7日学生进行毕业设计(论文)2016年4月中旬(根据期中教学检查文件执行)准备中期检查有关材料,学院自查 2016年4月下旬(根据期中教学检查文件执行)教务处及教学督导团进行中期抽查 2016年6月4日-6月10日 学院组织毕业设计(论文)答辩。