1. 毕业设计（论文）的内容和要求

1．文献查阅 掌握文献查阅的一般方法，学会使用计算机在中国期刊网、维普数据库、超星数字图书馆、美国化学学会（acs）数据库、ca、ei和sci等检索资源上查阅关于左旋葡聚糖酮的制备、气相色谱检测，气质联用法检测相关物质相关文献。

2．文献阅读及综述 阅读与课题相关的外文及中文文献，了解国内外的研究动态，撰写文献综述。

3．明确实验任务，拟定实验方案 根据所查阅文献的内容，确定实验内容及方案，拟定科学可行的研究计划。

2. 参考文献

中文文献：{1}汪东风．食品化学．北京：化学工业出版社，2009 {2}韩俊鹏. 纤维素的降解[J]. 煤炭与化工, 2011, 34(9):28-32. {4}隋先伟, 汪志, 阮仁祥,等. 左旋葡萄糖酮的研究综述[J]. 现代化工, 2010, 30(11):29-36. 外文文献： [ 3]HalpernY, RiferR, BroidoA.Levoglucosenone(1, 6-anhydro-3, 4-dideoxy-.DELTA.3-.beta.-D-pyranosen-2-one).Majorproduct oftheacid-catalyzedpyrolysisofceluloseandrelatedcarbohydrates [ J] .TheJournalofOrganicChemistry, 1973, 38(2):204 -209. [ 5]HalpernY, HoppeschJP.Amassspectrometrystudyoflevoglu- cosenone[ J] .TheJournalofOrganicChemistry, 1985, 50 (9): 1556 -1557. [ 6]OhnishiA, TakagiE, KatoK.Theopticalrotatorydispersionand circulardichroismoflevoglucosenone[J] .BuletinoftheChemical SocietyofJapan, 1975, 48(6):1959 -1960. [ 7]WitczakZJ, Levoglucosenone.Achiralbuildingblockwithanew perspective[ M] //ChemicalsandMaterialsfromRenewableRe- sources, Washington, DC:AmericanChemicalSociety, 2001:81 - 97. {8}WitczakZJ,ChhabraR,BoryczewskiD.Thiosugars:.Stereose-lectiveapproachtobeta-(12)-2,3-dideoxy-2-C-acetamidom-ethyl-2-S-thiodisaccharidesfromlevoglucosenone[ J] .Journalof CarbohydrateChemistry, 2000, 19(4 /5):543 -553. [9] MoriM, ChumanT, KatoK, etal.Astereoselectivesynthesisof ”natural” (4S, 6S, 7S)-sericornin, thesexpheromoneofcigarete betle, fromevoglucosenone[ J] .TetrahedronLeters, 1982, 23 {10}4593 -4596.WitczakZJ, LiY.NewStereoselectiveApproachto(-)-delta-multistriatin[ J] .TetrahedronLeters, 1995, 36(15):2595 -2598. [11]UrabeD,NishikawaT,IsobeM.Aneficienttotalsynthesisofopti-calyactivetetrodotoxinfromlevoglucosenone[ J] .Chemistry-anAsianJournal, 2006, 1(1/2):125 -135.□ {12}HalpernY,RiferR,BroidoA.Levoglucosenone(1,6-anhydro-3,4-dideoxy-.DELTA.3-.beta.-D-pyranosen-2-one).Majorproductoftheacid-catalyzedpyrolysisofceluloseandrelatedcarbohydrates[ J] .TheJournalofOrganicChemistry, 1973, 38(2):204 -209. {13}ShafizadehF, FurneauxRH, StevensonTT.Somereactionsoflevo-glucosenone[ J] .CarbohydrateResearch, 1979, 71(1):169 -191. [14]DobeleG,RossinskajaG,TelyshevaG,etal.Cellulosedehydrationanddepolymerizationreactionsduringpyrolysisinthepresenceofphosphoricacid[ J] .JournalofAnalyticalandAppliedPyrolysis,1999, 49(1 /2):307 -317. [ 15] DobeleG, MeierD, FaixO, etal.Volatileproductsofcatalyticflashpyrolysisofcelluloses[J] .JournalofAnalyticalandAppliedPyrol-ysis, 2001, 58:453 -463. [16] DobeleG, DizhbiteT, RossinskajaG, etal.Pre-treatmentofbiomas withphosphoricacidpriortofastpyrolysis:Apromisingmethodfor obtaining1, 6-anhydrosaccharidesinhighyields[ J] .JournalofAn-alyticalandAppliedPyrolysis, 2003, 68/69:197 -211. [17] DobeleG, RossinskajaG, DiazbiteT, etal.Applicationofcatalysts forobtaining1, 6-anhydrosaccharidesfromceluloseandwoodby fastpyrolysis[ J] .JournalofAnalyticalandAppliedPyrolysis,2005, 74(1 /2):401 -405. {18}WitczakZJ,NewStereoselectivefunctionalizationofcellulose-de-rivedpyrolysisderivatives:Levoglucosenoneanditsdimer[ M] // Materials, Chemicals, andEnergyfromForestBiomass, Washington DC:AmericanChemicalSociety, 2007:332 -349. {19}MarshalJ.Animprovedpreparationoflevoglucosenonefromcellu-lose[ M] .Iowa:IowaStateUniversityAmes, 2008. {20}Terri I G.Lesci D F.Analytical study onthe pyrolytic behaviour of cellulose in the presence of MCM-41 mesoporous materials[J].Journal of analytical and Applied Pyrolysis.2009,85(01):192-196. {21}Piotr R. Pyrolytic behavior of cellulose in presence of montmorillonite K10 as catalyst[J].Journal of analytical and Applied Pyrolysis,2012.9:115-122. {22}Fabbri D. Torri C.Baravelli V.Effect of zeolites and nanopowder metaloxides on the distribution of chiral anhydrosugars evolved from pyrolysis of cellulose :An analytical study[J].Journal of analytical and Applied Pyrolysis.2007.80(1):24-29 {23}Fu Q.Argyropoulos D S.Tilotta D C.et al.Understanding the pyrolysis of CCA-treated wood: PART Ц.Effect of phosphoric acid[J].Journal of analytical and Applied Pyrolysis.2008,82(1):140-144,

3. 毕业设计（论文）进程安排

起讫日期 设计（论文）各阶段工作内容 2016.12.-2017.1.1 文献查询和资料阅读 2017.1.1-2017.1.13 研究方案制定和开题报告写作 2017.2.21-2017.5.30 实验研究过程 2017.5.1-2017.5.15 中期检查、数据整理与处理、完善实验 2017.5.30-2017.6.8 论文写作与修改、成文 2017.6.9-2017.6.11 论文答辩